Chapter Optimization of the Synthesis Procedures of Graphene and Graphite Oxide (Record no. 38275)
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| 000 -LEADER | |
|---|---|
| fixed length control field | 02497naaaa2200301uu 4500 |
| 001 - CONTROL NUMBER | |
| control field | https://directory.doabooks.org/handle/20.500.12854/70408 |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER | |
| International Standard Book Number | 63752 |
| 024 7# - OTHER STANDARD IDENTIFIER | |
| Standard number or code | 10.5772/63752 |
| Terms of availability | doi |
| 041 0# - LANGUAGE CODE | |
| Language code of text/sound track or separate title | English |
| 042 ## - AUTHENTICATION CODE | |
| Authentication code | dc |
| 072 #7 - SUBJECT CATEGORY CODE | |
| Subject category code | TBN |
| Source | bicssc |
| 100 1# - MAIN ENTRY--PERSONAL NAME | |
| Personal name | Luis Valverde Palomino, José |
| Relationship | auth |
| 245 10 - TITLE STATEMENT | |
| Title | Chapter Optimization of the Synthesis Procedures of Graphene and Graphite Oxide |
| 260 ## - PUBLICATION, DISTRIBUTION, ETC. | |
| Name of publisher, distributor, etc. | InTechOpen |
| Date of publication, distribution, etc. | 2016 |
| 506 0# - RESTRICTIONS ON ACCESS NOTE | |
| Terms governing access | Open Access |
| Source of term | star |
| Standardized terminology for access restriction | Unrestricted online access |
| 520 ## - SUMMARY, ETC. | |
| Summary, etc. | The optimization of both the chemical vapor deposition (CVD) synthesis method to prepare graphene and the Improved Hummers method to prepare graphite oxide is reported. Copper and nickel were used as catalysts in the CVD-graphene synthesis, CH4 and H2being used as precursor gases. Synthesis variables were optimized according to a thickness value, calculated using a homemade Excel-VBA application. In the case of copper, the maximum thickness value was obtained for those samples synthesized at 1050°C, a CH4/H2 flow rate ratio of 0.07 v/v, a total flow of 60 Nml/min, and a time on stream of 10 min. In the case of nickel, a reaction temperature of 980°C, a CH4/H2 flow rate ratio of 0.07 v/v, a total flow of 80 Nml/min, and a time on stream of 1 min were required to obtain a high thickness value. On the other hand, the Improved Hummers method used in the synthesis of graphite oxide was optimized. The resultant product was similar to that reported in literature in terms of quality and characteristics but both time and cost of the synthesis procedure were considerably decreased. |
| 540 ## - TERMS GOVERNING USE AND REPRODUCTION NOTE | |
| Terms governing use and reproduction | Creative Commons |
| Use and reproduction rights | https://creativecommons.org/licenses/by/3.0/ |
| Source of term | cc |
| -- | https://creativecommons.org/licenses/by/3.0/ |
| 546 ## - LANGUAGE NOTE | |
| Language note | English |
| 650 #7 - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | Nanotechnology |
| Source of heading or term | bicssc |
| 653 ## - INDEX TERM--UNCONTROLLED | |
| Uncontrolled term | graphene, graphite oxide, CVD, Improved Hummers method, thickness value |
| 700 1# - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Romero Izquierdo, Amaya |
| Relationship | auth |
| 700 1# - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Sánchez Silva, MaríaLuz |
| Relationship | auth |
| 700 1# - ADDED ENTRY--PERSONAL NAME | |
| Personal name | del Prado Lavín López, María |
| Relationship | auth |
| 773 10 - HOST ITEM ENTRY | |
| Host Biblionumber | OAPEN Library ID: ONIX_20210602_10.5772/63752_275 |
| Control subfield | nnaa |
| 856 40 - ELECTRONIC LOCATION AND ACCESS | |
| Host name | www.oapen.org |
| Uniform Resource Identifier | <a href="https://library.oapen.org/bitstream/20.500.12657/49161/1/51090.pdf">https://library.oapen.org/bitstream/20.500.12657/49161/1/51090.pdf</a> |
| Access status | 0 |
| Public note | DOAB: download the publication |
| 856 40 - ELECTRONIC LOCATION AND ACCESS | |
| Host name | www.oapen.org |
| Uniform Resource Identifier | <a href="https://library.oapen.org/bitstream/20.500.12657/49161/1/51090.pdf">https://library.oapen.org/bitstream/20.500.12657/49161/1/51090.pdf</a> |
| Access status | 0 |
| Public note | DOAB: download the publication |
| 856 40 - ELECTRONIC LOCATION AND ACCESS | |
| Host name | www.oapen.org |
| Uniform Resource Identifier | <a href="https://directory.doabooks.org/handle/20.500.12854/70408">https://directory.doabooks.org/handle/20.500.12854/70408</a> |
| Access status | 0 |
| Public note | DOAB: description of the publication |
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